By J. W. Hylin
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Y. 10010, Telephone (212) 673-9797. Conversion of a Dohrmann Microcoulometric Gas Chromatograph to a Convenient and Rapid "Total Chloride" Unit by FRANCIS A. GuNTHER and ]AMES H. BARKLEY Department of Entomology University of California Citrus Research Center and Agricultural Experiment Station, Riverside, California In quantitative residue investigations of the persisting organochlorine pesticides in foodstuffs there is frequent need to establish magnitudes of the total organically bound chlorine present.
00). The 6% ether fraction of control orange rind samples, processed as described, produced no peaks in the area of interest. This same fraction from subject field-treated oranges, however, showed the glc presence of two compounds with retention times identical to those of 2,£ 1 - and £,£ 1 -Kelthane. When 2,£'- and £,£ 1 -Kelthanes were added to this fraction each corresponding peak height was increased with no indication of new doublet formation. When heptachlor was added, however, a new doublet was formed with the SF-96 and Apiezon L columns and distinct heptachlor and 2,£'-Kelthane peaks resulted when the QF-1-DC-200 column was used.
B. BARICLEY, R. C. BLINN, and D. E. , Stanford Research Inst. #V 2; 3 (1962). , ''Detennination of Endrin in Animal Tissues, Eggs, Butter, and Milk by Total Chloride Method", PP• 1-32, Aug. 13, 1956. 38 Contents CONVERSION OF A DOHRMANN MICROCOULOMETRIC GAS CHROMATOGRAPH TO A CONVENIENT AND RAPID "TOTAL CHLORIDE" UNIT by Francis A. Gunther and James H. Barkley .. .... .. 39 RESIDUAL NATURE OF CERTAIN ORGANOPHOSPHORUS INSECTICIDES IN GRAIN SORGHUM AND COASTAL BERMUDAGRASS by H. W. Dorough, N.
